Not until I have the general's head on a spear in my hand.
6 seconds sound clip from the Ninjutsu (1968) movie soundboard.
You can hear this line at 01:27:23 in the Blu-ray version of the movie.
Quote context
[...]
- Hmm, if you're able to get past the both of us, then Sher Ping Way will agree to fight you himself.
- Right.
- Did you bring the book with you?
- Release Mr. Chi first, only then will I hand over the book to you.
- Not until I have the general's head on a spear in my hand.
- Right!
[...]